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The Chrystal G. Tibbs Papers comprise over a half-century of documents pertaining to Tibbs's membership in various chapters of the Alpha Kappa Alpha Sorority and to the history of the sorority at large. Founded at Howard University in 1908, A.K.A. was the first sorority established by African-American women and currently has approximately 250,000 members. The collection's four series contain papers pertaining to Tibbs's personal participation in sorority activities (including those related to her tenure in various administrative posts), materials from several Michigan chapters, sorority publications, and audiovisual materials. In addition, the collection contains work done by Tibbs and family members to document the Powell, Webster, and Winchester family history.

The Chrystal G. Tibbs Papers comprise materials accumulated through Tibbs's participation in Alpha Kappa Alpha conferences, chapter meetings, and special interest groups at the local, state, regional, and national level over a span of fifty years. The activities of Michigan-based chapters are particularly well represented. Materials also include personal and professional documentation directly related to Tibbs and her immediate family. The collection is divided into four series: Personal Papers, Professional Career, Powell Family Papers, and Alpha Kappa Alpha Sorority.